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  Course Description
Course Name : Instrumental Analysis Lab

Course Code : KM 462

Course Type : Compulsory

Level of Course : First Cycle

Year of Study : 4

Course Semester : Spring (16 Weeks)

ECTS : 2

Name of Lecturer(s) : Prof.Dr. BİLGEHAN GÜZEL
Asst.Prof.Dr. SİBEL IRMAK
Prof.Dr. BİLGEHAN GÜZEL

Learning Outcomes of the Course : Introduce instrumental analysis devices
Learn these devices´ parts.
Learn how to prepare the given sample.
Learn how to use the instrument´s knowledge.
Learn qualitative and quantitative analysis practically.
Learn how to relate the chemistry knowledge with instrumental analysis.

Mode of Delivery : Face-to-Face

Prerequisites and Co-Prerequisites : None

Recommended Optional Programme Components : None

Aim(s) of Course : Instrumental anlysis experiments, their qualitative and quantitative analysis methods

Course Contents : To introduce instrumental methods wtih experiments

Language of Instruction : Turkish

Work Place : Laboratory


  Course Outline /Schedule (Weekly) Planned Learning Activities
Week Subject Student's Preliminary Work Learning Activities and Teaching Methods
1 To introduce UV spectrophotometry Related experiment should be studied before coming lab Presentation, Experiment with devices
2 Quantitative analysis of two components mixture with UV spectrometry Related experiment should be studied before coming lab Presentation, Experiment with devices
3 Absroption spectrums of aromatic compounds Related experiment should be studied before coming lab Presentation, Experiment with devices
4 Gas chromatography Related experiment should be studied before coming lab Presentation, Experiment with devices
5 Analysis with Gas chromatography-Mass spectrometer Related experiment should be studied before coming lab Presentation, Experiment with devices
6 Analysis with Infrared spectroscopy Related experiment should be studied before coming lab Presentation, Experiment with devices
7 High performance liquid chromatography Related experiment should be studied before coming lab Presentation, Experiment with devices
8 Midterm Related experiments should be studied before coming lab Exam
9 Analysis with ion chromatography Related experiment should be studied before coming lab Presentation, Experiment with devices
10 To introduce total organic carbon analysis device Related experiment should be studied before coming lab Presentation, Experiment with devices
11 Analysis with atomic absorption spectrometry Related experiment should be studied before coming lab Presentation, Experiment with devices
12 Magnetic susseptibility Related experiment should be studied before coming lab Presentation, Experiment with devices
13 Refractometry Related experiment should be studied before coming lab Presentation, Experiment with devices
14 Analysis with TGA device Related experiment should be studied before coming lab Presentation, Experiment with devices
15 Make up experiments Related experiment should be studied before coming lab Presentation, Experiment with devices
16/17 Final exam Related experiments should be studied before coming lab Exam


  Required Course Resources
Resource Type Resource Name
Recommended Course Material(s)  1. Skoog, D.A, Holler, F.J., Nieman, T.A.; Principles of Instrumental Analysis. 2. Erdik, E. (2007). Spectroscopic Methods in Organic Chemistry.
Required Course Material(s)  3. Silverstein, R.M., Bassler, G.C., Morrill, T.C (1991). Spectrometric Identification of Organic Compounds, fifth edition, John Wiley&Sons Inc., New York.


  Assessment Methods and Assessment Criteria
Semester/Year Assessments Number Contribution Percentage
    Mid-term Exams (Written, Oral, etc.) 1 95
    Homeworks/Projects/Others 1 5
Total 100
Rate of Semester/Year Assessments to Success 40
 
Final Assessments 100
Rate of Final Assessments to Success 60
Total 100

  Contribution of the Course to Key Learning Outcomes
# Key Learning Outcome Contribution*
1 Feel comfortable with chemistry knowledge and capable to make relation with practical applicaitons 5
2 Observe and analyze the developments, directions and needs of industires for sustainability 3
3 Acquire life long education capability 3
4 Have capability of reaching for information 4
5 Acknowledge about total quality and relating the knowledge from different disciplines 5
6 Have capability of evaluating the national sources for technology development 0
7 Have capability of transmitting the knowledge and relating different disciplines 4
8 Gain the ability to achieve new knowledge and technology 4
9 Learn problem solving methodolygy and creative thinking 3
10 Have capability of bringing together theory and practical applicaiton 4
11 Feel comfortable with laboratory studies 5
12 Follow the developments in chemistry industries 2
13 Monitor progress in the field of chemistry. 4
14 Have capability of team work and leadership 4
15 Acquire property of objective and critical view 0
* Contribution levels are between 0 (not) and 5 (maximum).

  Student Workload - ECTS
Works Number Time (Hour) Total Workload (Hour)
Course Related Works
    Class Time (Exam weeks are excluded) 14 3 42
    Out of Class Study (Preliminary Work, Practice) 14 1 14
Assesment Related Works
    Homeworks, Projects, Others 1 1 1
    Mid-term Exams (Written, Oral, etc.) 1 2 2
    Final Exam 1 2 2
Total Workload: 61
Total Workload / 25 (h): 2.44
ECTS Credit: 2